PQ Systems Knowledge Base

ST: What kind of set-up would you recommend for testing one instrument?

Revision Date: 2005-09-06

Problem:

It measures percent acidity. There are six analysts who use the instrument to test acids whose strengths range from 50% to nearly 100%. I could have each analyst run the same of several samples in triplicate. I could fix the sample weights + or - 0.1 gram.

Solution:

It depends on what you are trying to accomplish.  To some extent, R&R studies may not be appropriate. One objective would be to see how the gage accuracy varies over the relevant range (50% to 100%).  You can do this with a linearity study.  The major difference is that the parts used for the study are different products with values that range throughout the gage range, e.g., 55%, 65%, 75%, 85%, & 95%. You need reference values (true values) for each product. These can come from certified samples (like using gage blocks) or from using a "super" gage with better known accuracy.  Since you are using different products, the traditional R&R percentages do not mean anything.  However, if you wanted to test if the appraisers are measuring things differently, you could use more than one operator and check the operator bias and the operator uncertainty results. 

If you want to run a traditional R&R, I would suggest picking a concentration where most of the tests are run. You can use all six operators in the same study.  Given the previous results, I would suggest this as well, providings it does not overcomplicate the running of the tests.  Here the samples (5-10) need to come from one product, but have values typical of the total range of the product variation.  Two or three replications should work fine.  This would allow you to check the gages' ability to discriminate among the values for the product and to evaluate the performance of the operators.  Linearity could not be checked for the gage, however.

 

Gordon Constable, Ph.D.

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